Mined in Frechen, Germany, the quartz is mostly silicon dioxide with trace amounts of iron (Fe), titanium (Ti), sodium (Na) and calcium (Ca). The chemical composition was characterized using hydrofluoric acid dissolution, the resulting residue was analyzed. Sodium and calcium content were determined by flame photometry. Iron and titanium content were determined using spectrophotometric techniques.
BCR 66, 67, 69 and 70 were calibrated by gravimetric sedimentation and BCR 68 and 130 by a sieving technique by the BCR. The samples were also analyzed by TEM, electrical sensing zone, sieving and several sedimentation methods. A continuum of the weight distribution is provided for each sample. The density was determined by pyknometer and is approximately 2.6 g/cm3.
Results and methods are summarized in two detailed reports:
-
Certification Report on Reference Materials of Defined Particle Size, for BCR 66 through 70.
-
Certification Report on Reference Materials of Defined Particle Size, for BCR 130.
Both reports are included with the kit.*
Each individual bottle of quartz reference particles is accompanied by a Certificate of Measurement, which outlines measurement methods, chemical analysis data and instructions for use.
*The appropriate report will be included with orders of six or more kits (any combination) at no charge.